02779cam a22002774a 4500001001100000005001700011008004100028010001700069020002800086035001300114040001800127050002300145082001600168100004700184245011900231250001200350260003100362264003000393300004600423500005100469505189300520650002402413650002302437700001902460700002202479000003214520230921135531.0100715s2011    xx a     b    001 0 eng    a  2010027725  a9780123736284 :c$53.00  a16334273  aDLCcDLCdDLC00aQD79.C45bS66 201100a543/.852221 aSparkman, O. Davidq(Orrin David),d1942-.10aGas chromatography and mass spectrometry :ba practical guide /cO David Sparkman, Zelda Penton, Fulton G. Kitson.  a2nd ed.  aBoston :bElsevier,c2011.  aBoston :bElsevier,c2011  axix, 611 pages :billustrations ;c23 cm.  aIncludes bibliographical references and index.0 aThe fundamentals of GC/MS -- Introduction and history -- Gas chromatography -- The gc/ms interface -- Mass spectrometry instrumentation -- Mass spectral data interpretation -- Quantitation with GC/MS -- GC conditions, derivatization, and mass spectral interpretation -- Of specific compound types -- Acids -- Alcohols -- Aldehydes -- Amides -- Amines -- Amino acid -- Common contaminants -- Drugs and their metabolites -- Esters -- Ethers -- Fluorinated compounds -- Gases -- Glycols -- Halogenated compounds (other than fluorinated) -- Hydrocarbons -- Isocyanates -- Ketones -- Nitriles -- Nitroaromatics -- Nitrogen-containing heterocyclics -- Nucleosides (TMS derivatives) -- Pesticides -- Phenols -- Phosphorus compounds -- Plasticizers and other polymer additives (including phthalates) -- Prostaglandins (MO-TMS derivatives) -- Solvents and their impurities -- Steroids -- Sugars (monosaccharides) -- Sulfur compounds -- Appendices -- A definitions of terms related to gas chromatography -- B definitions of terms related to mass spectrometry -- C atomic masses and isotope abundances -- X+1 and x+2 values for ions containing atoms of C and H based on -- Isotope contributions -- E isotope peak patterns for ions containing atoms of Cl and/or Br -- F steps to follow in the determination of an elemental composition -- Based on isotope peak intensity ratios -- G derivatization in GC/MS -- H points of comparison of LC/MS vs GC/MS -- I list of available EI mass spectral databases -- J information required for reporting a GC/MS analysis -- K third-party software for use with GC/MS -- GC installation and maintenance -- Troubleshooting common GC problems -- N maintenance, operating tips, and troubleshooting for mass spectrometers -- O mixtures for determining mass spectral resolution -- P cross-index chart for GC stationary phases -- Q ions for determining unknown structures. 0aGas chromatography. 0aMass spectrometry.1 aPenton, Zelda.1 aKitson, Fulton G.