03236cam a22003614a 4500 0000032145 20230921135531.0 100715s2011 xx a b 001 0 eng 2010027725 9780123736284 : $53.00 16334273 DLC DLC DLC QD79.C45 S66 2011 543/.85 22 Sparkman, O. David (Orrin David), 1942-. Gas chromatography and mass spectrometry : a practical guide / O David Sparkman, Zelda Penton, Fulton G. Kitson. 2nd ed. Boston : Elsevier, 2011. Boston : Elsevier, 2011 xix, 611 pages : illustrations ; 23 cm. Includes bibliographical references and index. The fundamentals of GC/MS -- Introduction and history -- Gas chromatography -- The gc/ms interface -- Mass spectrometry instrumentation -- Mass spectral data interpretation -- Quantitation with GC/MS -- GC conditions, derivatization, and mass spectral interpretation -- Of specific compound types -- Acids -- Alcohols -- Aldehydes -- Amides -- Amines -- Amino acid -- Common contaminants -- Drugs and their metabolites -- Esters -- Ethers -- Fluorinated compounds -- Gases -- Glycols -- Halogenated compounds (other than fluorinated) -- Hydrocarbons -- Isocyanates -- Ketones -- Nitriles -- Nitroaromatics -- Nitrogen-containing heterocyclics -- Nucleosides (TMS derivatives) -- Pesticides -- Phenols -- Phosphorus compounds -- Plasticizers and other polymer additives (including phthalates) -- Prostaglandins (MO-TMS derivatives) -- Solvents and their impurities -- Steroids -- Sugars (monosaccharides) -- Sulfur compounds -- Appendices -- A definitions of terms related to gas chromatography -- B definitions of terms related to mass spectrometry -- C atomic masses and isotope abundances -- X+1 and x+2 values for ions containing atoms of C and H based on -- Isotope contributions -- E isotope peak patterns for ions containing atoms of Cl and/or Br -- F steps to follow in the determination of an elemental composition -- Based on isotope peak intensity ratios -- G derivatization in GC/MS -- H points of comparison of LC/MS vs GC/MS -- I list of available EI mass spectral databases -- J information required for reporting a GC/MS analysis -- K third-party software for use with GC/MS -- GC installation and maintenance -- Troubleshooting common GC problems -- N maintenance, operating tips, and troubleshooting for mass spectrometers -- O mixtures for determining mass spectral resolution -- P cross-index chart for GC stationary phases -- Q ions for determining unknown structures. Gas chromatography. Mass spectrometry. Penton, Zelda. Kitson, Fulton G. 7 cbc orignew 1 ecip 20 y-gencatlg 221018 acquire 2 shelf copies policy default claim1 2011-01-19 rd11 2010-07-16 re11 2011-06-10 to BCCD re11 2011-06-13 copy 2 added 20230822095114.0 9957 9957 0 0 0 0 cutlib cutlib 2023-09-21 0 QD 79.C45 SPA BK0091910 2023-09-21 00:00:00 C.047394 2023-09-21 BK