a practical guide Sparkman, O. David (Orrin David) 1942- creator Penton, Zelda. Kitson, Fulton G. text bibliography xx Boston Elsevier 2011 2nd ed. monographic eng

print

xix, 611 pages : illustrations ; 23 cm. The fundamentals of GC/MS -- Introduction and history -- Gas chromatography -- The gc/ms interface -- Mass spectrometry instrumentation -- Mass spectral data interpretation -- Quantitation with GC/MS -- GC conditions, derivatization, and mass spectral interpretation -- Of specific compound types -- Acids -- Alcohols -- Aldehydes -- Amides -- Amines -- Amino acid -- Common contaminants -- Drugs and their metabolites -- Esters -- Ethers -- Fluorinated compounds -- Gases -- Glycols -- Halogenated compounds (other than fluorinated) -- Hydrocarbons -- Isocyanates -- Ketones -- Nitriles -- Nitroaromatics -- Nitrogen-containing heterocyclics -- Nucleosides (TMS derivatives) -- Pesticides -- Phenols -- Phosphorus compounds -- Plasticizers and other polymer additives (including phthalates) -- Prostaglandins (MO-TMS derivatives) -- Solvents and their impurities -- Steroids -- Sugars (monosaccharides) -- Sulfur compounds -- Appendices -- A definitions of terms related to gas chromatography -- B definitions of terms related to mass spectrometry -- C atomic masses and isotope abundances -- X+1 and x+2 values for ions containing atoms of C and H based on -- Isotope contributions -- E isotope peak patterns for ions containing atoms of Cl and/or Br -- F steps to follow in the determination of an elemental composition -- Based on isotope peak intensity ratios -- G derivatization in GC/MS -- H points of comparison of LC/MS vs GC/MS -- I list of available EI mass spectral databases -- J information required for reporting a GC/MS analysis -- K third-party software for use with GC/MS -- GC installation and maintenance -- Troubleshooting common GC problems -- N maintenance, operating tips, and troubleshooting for mass spectrometers -- O mixtures for determining mass spectral resolution -- P cross-index chart for GC stationary phases -- Q ions for determining unknown structures. O David Sparkman, Zelda Penton, Fulton G. Kitson. Includes bibliographical references and index. Gas chromatography Mass spectrometry QD79.C45 S66 2011 543/.85 9780123736284 : 2010027725 DLC 100715 20230921135531.0 0000032145